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3-Phenoxybenzyl alcohol → 3-Phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Phenoxybenzyl alcohol | HCID 26295 | — |
| 反応物 | Methyl 2-(4-chlorophenylamino)-3-methylbutanimidate | HCID 12767220 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 3-Phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate | HCID 12767221 | — |
反応手順
A solution of 2.25 g (10 mmol) of methyl 2-(4-chlorophenylamino)-3-methylbutanimidate and 4.00 g (20 mmol) of 3-phenoxybenzyl alcohol is heated with continuous removal of methanol. Upon cessation of methanol evolution, there is obtained an oil, 3-phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04254264 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-25c9c6c8c5294111bda856bf486330e4 |
| 出典メモ | uspto-grants-1981_03 |