Lactic Acid → HCID 70568603、化合物
反応式
[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([CH2:9][C:10]2[CH:15]=[C:14]([O:16][CH3:17])[C:13]([C:18]([CH3:20])=[CH2:19])=[C:12]([O:21][CH3:22])[CH:11]=2)=[CH:4][N:3]=1.[C:23]([OH:28])(=[O:27])[CH:24]([CH3:26])[OH:25]>O>[C:23]([OH:28])(=[O:27])[CH:24]([CH3:26])[OH:25].[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([CH2:9][C:10]2[CH:11]=[C:12]([O:21][CH3:22])[C:13]([C:18]([CH3:20])=[CH2:19])=[C:14]([O:16][CH3:17])[CH:15]=2)=[CH:4][N:3]=1参加物
4
実験手順
4.5 G. of 2,4-diamino-5-(4-isopropenyl-3,5-dimethoxybenzyl)-pyrimidine and 1.9 g. of 72.5% lactic acid were dissolved in 250 ml. of water. The solution was filtered, concentrated to half volume, cooled and the crystalline 2,4-diamino-5-(4-isopropenyl-3,5-dimethoxybenzyl)-pyrimidine lactate, melting point 287°-290° C. (decomposition), was removed by filtration under suction.
後処理
- filtrationThe solution was filtered
- concentrationconcentrated to half volume