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HRID 1272397作成日:2026年10月27日

Aniline → Methanimidic acid, N-phenyl-, ethyl ester

https://huagongshe.com/reaction/1272397

反応式

関与物質

役割名称HCID仕込み量
反応物AnilineHCID 6115—
反応物Ethyl orthoformateHCID 31214—
反応物N,N'-DiphenylformamidineHCID 94888—
生成物Methanimidic acid, N-phenyl-, ethyl esterHCID 111236—

反応手順

The synthesis is achieved in three steps. The first step is the preparation of N,N′-diphenyl formamidine (by the reaction of aniline with triethyl orthoformate). This intermediate is then further reacted with triethyl orthoformate to produce ethyl N-phenylimidoformate. The final step is the reaction of ethyl phenylimidoformate with 4-aminostyrene to give the product.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07208557B2
出典データセットuspto-grants-2007_04
ORD IDord-1ef5853adf0c4154b000c2a12196db5b
出典メモuspto-grants-2007_04