化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → Methanimidic acid, N-phenyl-, ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Ethyl orthoformate | HCID 31214 | — |
| 反応物 | N,N'-Diphenylformamidine | HCID 94888 | — |
| 生成物 | Methanimidic acid, N-phenyl-, ethyl ester | HCID 111236 | — |
反応手順
The synthesis is achieved in three steps. The first step is the preparation of N,N′-diphenyl formamidine (by the reaction of aniline with triethyl orthoformate). This intermediate is then further reacted with triethyl orthoformate to produce ethyl N-phenylimidoformate. The final step is the reaction of ethyl phenylimidoformate with 4-aminostyrene to give the product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07208557B2 |
| 出典データセット | uspto-grants-2007_04 |
| ORD ID | ord-1ef5853adf0c4154b000c2a12196db5b |
| 出典メモ | uspto-grants-2007_04 |