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Sodium Bicarbonate → 4-Chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1yl)-butan-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 反応物 | 4-Chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1(imidazol-1-yl)-butan-2-one naphthalene-1,5-disulphonate | HCID 20286594 | — |
| 生成物 | 4-Chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1yl)-butan-2-one | HCID 20286595 | — |
反応手順
The 4-chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1-yl)-butan-2-one naphthalene-1,5-disulphonate obtained according to Example 4 was neutralized with sodium bicarbonate solution. 4-Chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1yl)-butan-2-one of melting point 97°-99° C. was obtained quantitatively.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04255434 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-828bbc97c0e948c6a7636eca3a9ec487 |
| 出典メモ | uspto-grants-1981_03 |