化工社化工社 化学情報印刷レポート · 研究参考用
Chloride → 2-Methyl-3,4,6-trifluorobenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chloride | HCID 312 | — |
| 反応物 | 2-Methyl-3,4,6-trifluorobenzoic acid | HCID 10130305 | — |
| 生成物 | 2-Methyl-3,4,6-trifluorobenzoyl chloride | HCID 15007607 | — |
反応手順
To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723648 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-141b4f862c4146f6950ca566cd749152 |
| 出典メモ | uspto-grants-1998_03 |