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1,4-Dimethyl L-aspartate → N-[2-[1,1-Dimethylethoxycarbonylamino]thiazol-4-yl]acetyl-L-aspartic acid, dimethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,4-Dimethyl L-aspartate | HCID 111207 | — |
| 反応物 | 2-(2-((tert-Butoxycarbonyl)amino)thiazol-4-yl)acetic acid | HCID 15480006 | — |
| 生成物 | N-[2-[1,1-Dimethylethoxycarbonylamino]thiazol-4-yl]acetyl-L-aspartic acid, dimethyl ester | HCID 86756129 | — |
反応手順
The subtitle compound was prepared from 2-[1,1-dimethylethoxycarbonylamino]thiazol-4-ylacetic acid (Chem. Pharm. Bull. 1993, 41, 758) (1.0 g) and L-aspartic acid dimethyl ester (1.15 g) according to the method of example 10 step (i). Yield 1.36 g. Used directly in the next step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06162808 |
| 出典データセット | uspto-grants-2000_12 |
| ORD ID | ord-42bf9ceed13f4a34bb0ec946f8ea67d9 |
| 出典メモ | uspto-grants-2000_12 |