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p-Toluenesulfonic acid → Sodium 4-methylbenzenesulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-Toluenesulfonic acid | HCID 6101 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 4-(6-Piperidinohexyl)3,5-dioxomorpholine | HCID 12796195 | — |
| 反応物 | 4-(6-Piperidinohexyl)-3,5-dioxomorpholine p-toluenesulfonate | HCID 12796196 | — |
| 生成物 | Sodium 4-methylbenzenesulfonate | HCID 3720192 | — |
| 生成物 | Sodium [2-(6-piperidinohexyl)amino-2-oxoethoxy]acetate | HCID 23686820 | — |
反応手順
Preparation in situ from 4-(6-piperidinohexyl)-3,5-dioxomorpholine-p-toluenesulfonate. 43 milligrams (0.095 millimole) of 4-(6-piperidinohexyl)-3,5-dioxomorpholine.p-toluenesulfonate (prepared as described in Example IX) was dissolved in 2 milliliters of 0.1 N sodium hydroxide (0.2 millimole) to obtain an aqueous solution of sodium [2-(6-piperidinohexyl)amino-2-oxoethoxy]acetate and sodium tosylate. The solution had the following spectral characteristics:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04256891 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-33a23f1db82a44a883dbaabee6730d1b |
| 出典メモ | uspto-grants-1981_03 |