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EDTA disodium salt → Edetate Disodium

HRID 1277583
ノート
印刷プレビュー

反応式

HRID 1277583 の反応式
[CH2:1]([CH2:11][N:12]([CH2:17][C:18]([O-:20])=[O:19])[CH2:13][C:14]([OH:16])=[O:15])[N:2]([CH2:7][C:8]([OH:10])=[O:9])[CH2:3][C:4]([O-:6])=[O:5].[Na+:21].[Na+].C(=O)(O)[O-:24].[Na+]>O>[OH2:5].[OH2:24].[CH2:11]([CH2:1][N:2]([CH2:7][C:8]([O-:10])=[O:9])[CH2:3][C:4]([OH:6])=[O:5])[N:12]([CH2:17][C:18]([OH:20])=[O:19])[CH2:13][C:14]([O-:16])=[O:15].[Na+:21].[Na+:21]
参加物実験手順後処理出典と根拠反応ノート

参加物

4

反応物 2

HCID 8759EDTA disodium saltHCID 516892Sodium Bicarbonate

生成物 1

HCID 636371Edetate Disodium

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

The disodium edetate was dissolved in the water. The cobaltous carbonate was added slowly with stirring. Gradual evolution of bubbles occurred after enough of the metal salt had been added to raise the pH to roughly 5. At that point, the insoluble material began to disappear more rapidly. After all of the bubbling had stopped, the liquid was stirred for approximately 15 minutes, and then the sodium bicarbonate was added slowly, with ample reaction time before further addition. The reaction was complete when a clear pink solution was obtained.

後処理

  1. additionhad been added
  2. temperatureto raise the pH to roughly 5
  3. stirringthe liquid was stirred for approximately 15 minutes
  4. customwas obtained

出典と根拠

ORDレコード
ord-014b86c514754142a83cc7b425e408ae
出典データセット
uspto-grants-1981_07
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04278610

反応ノート

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