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3-(Dimethylamino)-1-(furan-3-yl)prop-2-en-1-one → Ethyl 7-(3-Furyl)pyrazolo[1,5-a]pyrimidine-3-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Dimethylamino)-1-(furan-3-yl)prop-2-en-1-one | HCID 1474655 | — |
| 反応物 | HCID 178469928 | HCID 178469928 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Ethyl 7-(3-Furyl)pyrazolo[1,5-a]pyrimidine-3-carboxylate | HCID 21163074 | — |
反応手順
A mixture of 0.01 mole of 3-dimethylamino-1-(3-furyl)-2-propen-1-one and 0.01 mole of ethyl 3-aminopyrazole-4-carboxylate in glacial acetic acid is heated at reflux temperature for 6 hours. The product is isolated as described for Example 1 to give the product of the example.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04281000 |
| 出典データセット | uspto-grants-1981_07 |
| ORD ID | ord-ead09c32b3674bc28a4200631fcc659a |
| 出典メモ | uspto-grants-1981_07 |