化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Bromide → 4-Methylisoquinolin-7-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | 7-Methoxy-4-methylisoquinoline | HCID 20523203 | — |
| 生成物 | 4-Methylisoquinolin-7-ol | HCID 20523221 | — |
反応手順
A mixture of 17.3 g. (0.1 mole) of 7-methoxy-4-methylisoquinoline and 100 ml. of 48% hydrobromic acid is refluxed for sixteen hours and evaporated in vacuo. The residue is dissolved in water, neutralized with ammonium hydroxide and filtered to yield 7-hydroxy-4-methylisoquinoline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04258049 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-948ffba10f3c482688859b302143d3f1 |
| 出典メモ | uspto-grants-1981_03 |