化工社化工社 化学情報印刷レポート · 研究参考用
Hydrazine → 1-Cyclohexyl-1-phenyl-hydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrazine | HCID 9321 | — |
| 反応物 | N-Cyclohexylaniline | HCID 74567 | — |
| 反応物 | Aluminium lithium hydride | HCID 21226445 | — |
| 反応物 | N-Cyclohexyl-N-phenylnitrous amide | HCID 23471014 | — |
| 生成物 | 1-Cyclohexyl-1-phenyl-hydrazine | HCID 12866328 | — |
反応手順
N-Cyclohexyl-N-nitrosoaniline, prepared from N-cyclohexylaniline by the method described in Example 1 was subsequently reduced to the hydrazine by the lithium aluminum hydride method described in Example 4. 1-Cyclohexyl-1-phenyl hydrazine distilled at 120°-150° C./0.2 mm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04258059 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-1359a50870784657a2321d5ed8fa712e |
| 出典メモ | uspto-grants-1981_03 |