化工社化工社 化学情報印刷レポート · 研究参考用
Water → HCID 15571500、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 反応物 | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| 反応物 | 1-Cyclohexyl-1-phenyl-hydrazine | HCID 12866328 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | HCID 15571500 | HCID 15571500 | — |
反応手順
A mixture of 8.5 g (0.045 mol) 1-cyclohexyl-1-phenyl hydrazine in 50 ml isopropanol and 4.7 g (0.045 mol) sodium bicarbonate was stirred and chilled. Addition of 11.36 g (0.045 mol) 3-sulfamoyl-4-chlorobenzoyl chloride was made in several portions. The mixture was stirred for 2 hours at room temperature and for 2.5 hours at 40°-50° C. Dilution of the reaction mixture with water yielded a solid material which was recrystallized from aqueous ethanol. M.P. 216°-217° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04258059 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-3b94d622df534980ab8e261ba30bb99e |
| 出典メモ | uspto-grants-1981_03 |