化工社化工社 化学情報印刷レポート · 研究参考用
Dioctadecylamine → HCID 20433003、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dioctadecylamine | HCID 66989 | — |
| 反応物 | Ethyl 4-bromobutyrate | HCID 76300 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | HCID 20433003 | HCID 20433003 | 58.2% |
反応手順
A solution of dioctadecylamine (5.2 g., 0.01 mole), ethyl 4-bromobutyrate (1.95 g., 0.01 mole) and toluene (50 ml.) is heated at reflux for sixteen hours, then cooled and concentrated in vacuo to a semi-solid oil. The oil is triturated with ethylacetate, filtered, and the filtrate washed with water, then dried (Na2SO4). Removal of the solvent gives the product as an oil (3.7 g.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04258061 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-24c64bf11f244c4e8505596e5ea82237 |
| 出典メモ | uspto-grants-1981_03 |