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5-Chloro-2-methylphenyl isothiocyanate → 1-(5-Chloro-2-methyl-phenyl)-3-(4-methyl-thiazol-2-yl)-thiourea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Chloro-2-methylphenyl isothiocyanate | HCID 29519 | — |
| 反応物 | 2-Amino-4-methylthiazole | HCID 74143 | — |
| 生成物 | 1-(5-Chloro-2-methyl-phenyl)-3-(4-methyl-thiazol-2-yl)-thiourea | HCID 9835872 | 95% |
反応手順
Prepared using Method B from 4.5 g (24.5 mmol) of 5-chloro-2-methyl-phenyl isothiocyanate and 2.8 g (24.5 mmol) of 2-amino4-methylthiazole to give 4.8 g of title compound as an off- white solid (95% yield, m.p. 188° C.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06455566B1 |
| 出典データセット | uspto-grants-2002_09 |
| ORD ID | ord-2d91d85150d440ce946d7d37307818ff |
| 出典メモ | uspto-grants-2002_09 |