Phosgene → HCID 21453101、化合物
反応式
[C:1]([Cl:4])(=[O:3])[NH2:2].[CH:5]([N:7]1[CH2:12][CH2:11][CH2:10]N[C:8]1=[O:13])=[O:6].C(Cl)(Cl)=O>>[Cl:4][C:1]([N:2]1[CH2:10][CH2:11][CH2:12][N:7]([CH:8]=[O:13])[C:5]1=[O:6])=[O:3]参加物
4
実験手順
This carbamic acid chloride was produced as described in Example 27 B from 5 parts by weight of 1-formyl-2-oxo-1,3-diaza-cyclohexane and 6 parts by weight of phosgene. The substance, an oil, was used without further purification for the production of the penicillin of Example 35 A. IR-bands at 1790, 1685, 1300 and 1165 cm-1.
後処理
- customThe substance, an oil, was used without further purification for the production of the penicillin of Example 35 A
出典と根拠
- ORDレコード
- ord-318c7da8b8e8447cbe524aaaf599879d
- 出典データセット
- uspto-grants-1976_08
- 特許番号
- US03972869
反応ノート
読み込み中…