Ethanol → HCID 68122098、化合物
反応式
[C:1]1([CH:7]([CH:12]2[CH2:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH2:13]2)[CH2:8][CH2:9][CH2:10]Br)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[NH:22][CH2:23][CH2:24][CH3:25].[CH2:26](O)C>>[C:1]1([C:7]([NH:22][CH2:23][CH2:24][CH3:25])([CH:12]2[CH2:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH2:13]2)[CH2:8][CH2:9][CH2:10][CH3:26])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1参加物
4
反応条件
- 温度
- 100 °C
実験手順
A solution of 1-phenyl-1-(2-indanyl)-4bromobutane in ethanol was stirred at room temperature while methylpropylamine was added. The reaction mixture was stirred several hours at about 100°C. After cooling the reaction mixture to room temperature, the solvent was removed under reduced pressure, affording 1-phenyl-1-(2-indanyl)-4-methyl-n-propylaminobutane.