2,3,6-Trichloro-5-(chloromethyl)pyridine → 2,5,6-Trichloropyridine-3-carboxaldehyde

反応式

[Cl:1][C:2]1[C:7]([CH:8]=[O:9])=[CH:6][CH:5]=[C:4]([Cl:10])[N:3]=1.[Cl:11]C1C(CCl)=CC(Cl)=C(Cl)N=1>>[Cl:1][C:2]1[C:7]([CH:8]=[O:9])=[CH:6][C:5]([Cl:11])=[C:4]([Cl:10])[N:3]=1

参加物

反応物 2

HCID 122578712,3,6-Trichloro-5-(chloromethyl)pyridine

HCID 122593832,6-Dichloropyridine-3-carbaldehyde

生成物 1

HCID 122593852,5,6-Trichloropyridine-3-carboxaldehyde

実験手順

Obtained analogously to the process described for 2,6-dichloropyridine-3-aldehyde, using 2,5,6-trichloro-3-chloromethylpyridine instead of 2,6-dichloro-3-chloromethylpyridine.

後処理

customObtained analogously to the process

出典と根拠

ORDレコード: ord-897fee2d09b5474696a9e53f680ff20b
出典データセット: uspto-grants-1976_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US03974166

反応ノート

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