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Iodine → titanium(III) trichloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Iodine | HCID 807 | — |
| 反応物 | Diisopentyl ether | HCID 10989 | — |
| 反応物 | titanium(III) trichloride | HCID 10313229 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | titanium(III) trichloride | HCID 10313229 | — |
| 生成物 | I2 di-isoamyl ether | HCID 131712143 | — |
反応手順
Titanium trichloride composition (A) of 11.0 g was suspended in 55 ml of toluene and iodine and di-isoamyl ether were added in amounts to give a molar ratio of titanium trichloride composition (A)/I2 /di-isoamyl ether of 1.0/0.1/1.0 and then reacted at 80° C. for one hour to obtain titanium trichloride solid catalyst. This catalyst is referred to as titanium trichloride solid catalyst (II).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04259461 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-54247050930040fab4b17de526a68ef3 |
| 出典メモ | uspto-grants-1981_03 |