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Hydrochloric Acid → molybdenum N,N-dimethylaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N,N-Dimethylaniline | HCID 949 | — |
| 反応物 | Azanium bis(dioxido(dioxo)molybdenum) | HCID 21895884 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | molybdenum N,N-dimethylaniline | HCID 131710929 | — |
反応手順
N,N-dimethylaniline molybdate having a 2/1 molybdenum/N,N-dimethylaniline molar ratio was prepared in the presence of HCl as follows. 10 grams of N,N-dimethylaniline, 16.26 grams of a 37 wt.% aqueous HCl solution, and 250 ml water were dissolved together and heated to reflux in a 500 ml round-bottomed flask equipped with a water-cooled condenser. 28.05 grams of ammonium dimolybdate was dissolved in 52 ml hot water and then added to the first solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04259491 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-fee8ae2b43064c838c7c11ff8310f491 |
| 出典メモ | uspto-grants-1981_03 |