化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Molybdenum hexamethylenetetramine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Hexamethylenetetramine | HCID 4101 | — |
| 反応物 | Azanium bis(dioxido(dioxo)molybdenum) | HCID 21895884 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Molybdenum hexamethylenetetramine | HCID 131710930 | — |
反応手順
Hexamethylenetetramine molybdate having a 2/1 molybdenum/hexamethylenetetramine molar ratio was prepared in the presence of HCl as follows. 10 grams of hexamethylenetetramine, 14.05 grams of a 37 wt.% aqueous HCl solution, and 100 ml water were dissolved together and heated to reflux in a 500 ml round-bottomed flask equipped with a stirrer and water-cooled condenser. 24.24 grams ammonium dimolybdate was dissolved in 50 ml hot water. The second solution was added to the first solution, and a thin white precipitate formed rapidly.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04259491 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-b16b796b77884071a48d43a6d9e1e2ca |
| 出典メモ | uspto-grants-1981_03 |