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Hydrochloric Acid → Molybdenum 2,2,4-trimethyl decahydroquinoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Azanium bis(dioxido(dioxo)molybdenum) | HCID 21895884 | — |
| 反応物 | 2,2,4-Trimethyldecahydroquinoline | HCID 22628786 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Molybdenum 2,2,4-trimethyl decahydroquinoline | HCID 131710931 | — |
反応手順
2,2,4-Trimethyl decahydroquinoline molybdate having a 2/1 molybdenum/2,2,4-trimethyl decahydroquinoline molar ratio was prepared as follows. 10 grams 2,2,4-trimethyl decahydroquinoline, 16.30 grams of a 37 wt.% aqueous HCl solution and 250 ml water were dissolved together and heated to reflux in a 500 ml round-bottomed flask equipped with a stirrer and water-cooled condenser. 28.12 grams ammonium dimolybdate was dissolved in 50 ml hot water. The second solution was added to the first solution. A yellow precipitate formed immediately.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04259491 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-60ebefb24ff74d1690c3e9d29862484a |
| 出典メモ | uspto-grants-1981_03 |