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Trimethylamine → N-Octylisostearamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trimethylamine | HCID 1146 | — |
| 反応物 | Octylamine | HCID 8143 | — |
| 反応物 | 16-Methylheptadecanoic Acid | HCID 21859 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | Heptadecanoyl chloride, 16-methyl- | HCID 118402 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | N-Octylisostearamide | HCID 20150929 | — |
反応手順
Isostearoyl chloride, prepared from 20 g isostearic acid, 10.1 g thionyl chloride and 0.2 ml dimethyl formamide, according to the procedure of Example 1, is added to 11 g (0.09 mole) n-octylamine and 10 g (0.10 mole) trimethylamine in 100 ml ether. The reaction mixture is treated in accordance with the procedure of Example 2, yielding 22 g of an amber oil, which exhibits infrared spectra values typical of a secondary amide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04563288 |
| 出典データセット | uspto-grants-1986_01 |
| ORD ID | ord-3a39ca19a7214b18927cf17f5e1fbe8e |
| 出典メモ | uspto-grants-1986_01 |