化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Acifluorfen sodium
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Acifluorfen | HCID 44073 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | Acifluorfen sodium | HCID 44072 | 87.9% |
反応手順
5-(2-chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (3.0 g, 0.0083 mole) is dissolved in iso-propyl alcohol (20 ml) and a solution of 50% aqueous sodium hydroxide (0.644 g, 0.0083 mole) is added dropwise and the reaction mixture stirred for 1 hour before removing the solvent and water under vacuum at 0.2 mm overnight to afford 2.8 g of sodium 5-(2-chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04259510 |
| 出典データセット | uspto-grants-1981_03 |
| ORD ID | ord-042ebac77fc7400a9b466bd13adc6bac |
| 出典メモ | uspto-grants-1981_03 |