化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Sodium Dilysine Succinate Hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Succinic Acid | HCID 1110 | — |
| 反応物 | Sodium Succinate | HCID 9020 | — |
| 反応物 | Lysine Monohydrate | HCID 16211825 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sodium Dilysine Succinate Hydrochloride | HCID 86749085 | — |
反応手順
12 grams of L-lysine monohydrate is dissolved in 20 ml of water to which 6.0 ml of concentrated hydrochloric acid has been added. 2.964 grams of disodium succinate is added to neutralize some of the excess hydrochloric acid and 2.16 grams of succinic acid are added with mixing until effervescence ceases and all solids are dissolved. The solution is dried in a 110° C. oven until solids begin to form when cooled to room temperature. After 15 to 30 minutes solids form and are collected.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05464651 |
| 出典データセット | uspto-grants-1995_11 |
| ORD ID | ord-aa57a6c4c6e742af843ffca8738af246 |
| 出典メモ | uspto-grants-1995_11 |