Water → HCID 6404487、化合物

反応式

[C:1]1([C:7]2[CH:8]=[C:9]([C:14]([NH2:16])=O)[C:10](=O)[NH:11][N:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.O.P(Cl)(Cl)([Cl:20])=O>>[Cl:20][C:10]1[N:11]=[N:12][C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[CH:8][C:9]=1[C:14]#[N:16]

参加物

反応物 3

HCID 962Water

HCID 24813Phosphorus oxychloride

HCID 14753284D-083

生成物 1

HCID 6404487HCID 6404487、化合物

反応条件

温度: 80 °C

実験手順

1.5 g of the product obtained in Example 1 are dissolved in 20 ml of phosphorus oxychloride and the solution is then heated at 80° C. for 5 hours. The mixture is poured into 50 ml of water. A precipitate appears, which is filtered off and dried.

後処理

filtrationwhich is filtered off
customdried

出典と根拠

ORDレコード: ord-49d408cfb7874a49b5f9627ff0f2af9a
出典データセット: uspto-grants-1986_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04565814

反応ノート

読み込み中…