Ethanol, 2-fluoro-2,2-dinitro- → 1-Fluoro-1,1,5-trinitro-3-oxa-5azahexane

HRID 1285559

反応式

HRID 1285559 の反応式
FC(F)(F)C(O[CH2:6][N:7]([N+:9]([O-:11])=[O:10])[CH3:8])=O.[F:14][C:15]([N+:21]([O-:23])=[O:22])([N+:18]([O-:20])=[O:19])[CH2:16][OH:17]>>[F:14][C:15]([N+:21]([O-:23])=[O:22])([N+:18]([O-:20])=[O:19])[CH2:16][O:17][CH2:6][N:7]([N+:9]([O-:11])=[O:10])[CH3:8]

参加物

3

反応物 2

HCID 28189Ethanol, 2-fluoro-2,2-dinitro-HCID 13352131Acetic acid, trifluoro-, (methylnitroamino)methyl ester

生成物 1

HCID 133521331-Fluoro-1,1,5-trinitro-3-oxa-5azahexane

実験手順

reacting one mole of 2-nitro-2-azapropyl trifluoroacetate with one mole of 2-fluoro-2,2-dinitroethanol in a polar solvent at a temperature of from 0° C. to 40° C. to form 1-fluoro-1,1,5-trinitro-3-oxa-5azahexane, wherein the reaction is run under vacuum to remove trifluoroacetic acid generated by the reaction; and

後処理

  1. customof from 0° C. to 40° C.

出典と根拠

ORDレコード
ord-45804309d9454f8fb4d6d054f98606be
出典データセット
uspto-grants-1986_01
特許番号
US04567296

関連ノート

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