関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Decane, 1-isothiocyanato- | HCID 90535 | — |
| 反応物 | 4-Chloro-2-isothiocyanatopyridine | HCID 21508905 | — |
| 生成物 | 8-Chloro 3-(n-decyl) pyrido (1,2-a) 1,3,5-triazine-2,4-dithione | HCID 56607191 | — |
反応手順
0.511 G. of 4-Chloro-2-pyridyl isothiocyanate and 1.8 g. of n-decylisothiocyanate are combined and heated at 85° C. for 20 hours. The temperature is lowered to 75° C. and continued for 8 days. The reaction mixture is cooled, triturated with ether, filtered, washed with water and dried affording 8-chloro 3-(n-decyl) pyrido (1,2-a) 1,3,5-triazine-2,4-dithione m.p. 153°-155° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US03984549 |
|---|
| 出典データセット | uspto-grants-1976_10 |
|---|
| ORD ID | ord-e28dbc71cf6e40518f37c7328ca7a664 |
|---|
| 出典メモ | uspto-grants-1976_10 |
|---|
