化工社化工社 化学情報印刷レポート · 研究参考用
4-Methoxyphenylhydrazine hydrochloride → 3-Phthalimido-6-methoxy-1,2,3,4-tetrahydrocarbazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxyphenylhydrazine hydrochloride | HCID 2723904 | — |
| 反応物 | 2-(4-oxocyclohexyl)-2,3-dihydro-1H-isoindole-1,3-dione | HCID 11998391 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3-Phthalimido-6-methoxy-1,2,3,4-tetrahydrocarbazole | HCID 10807524 | 93.5% |
反応手順
Reaction of 4-methoxyphenyl hydrazine hydrochloride (0.87 g, 5.0 mmol) with 4-phthalimido-cyclohexanone (1.22 g, 5.0 mmol) in ethanol (20 ml) heated under reflux for 2 hr, followed by cooling and removal of the precipitated solid by filtration gave 3-phthalimido-6-methoxy-1,2,3,4-tetrahydrocarbazole (1.62 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05464864 |
| 出典データセット | uspto-grants-1995_11 |
| ORD ID | ord-2fe2b57280cf4d178a630ea8ac6bf48e |
| 出典メモ | uspto-grants-1995_11 |