Benzyl Bromide → HCID 21506015、化合物
反応式
N[C:2]1[CH:3]=[C:4]([CH:8]=[C:9](S(=O)(=O)N)[C:10]=1NC1C=CC=CC=1)[C:5](O)=O.[NH2:22][C:23]1[CH:24]=[C:25]([CH:29]=[C:30]([S:39](=[O:48])(=[O:47])[NH:40][C:41]2[CH:46]=[CH:45][CH:44]=[CH:43][CH:42]=2)[C:31]=1[NH:32][C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)[C:26]([OH:28])=[O:27].[CH2:49](Br)[C:50]1C=CC=CC=1>>[CH2:49]([O:27][C:26](=[O:28])[C:25]1[CH:29]=[C:30]([S:39](=[O:48])(=[O:47])[NH:40][C:41]2[CH:46]=[CH:45][CH:44]=[CH:43][CH:42]=2)[C:31]([NH:32][C:33]2[CH:34]=[CH:35][CH:36]=[CH:37][CH:38]=2)=[C:23]([NH:22][CH2:5][C:4]2[CH:8]=[CH:9][CH:10]=[CH:2][CH:3]=2)[CH:24]=1)[CH3:50]参加物
4
実験手順
By replacing, in Example 52 A, 3-amino-4-anilino-5-sulphamyl-benzoic acid (2 g) by 3-amino-4-anilino-5-phenylsulphamyl-benzoic acid (4.4 g) and increasing the amount of benzyl bromide to 3.9 g, ethyl-4-anilino-3-benzylamino-5-phenylsulphamyl-benzoate was obtained with a melting point of 166°-167° C.
出典と根拠
- ORDレコード
- ord-de36ccdea9c544978a9e0c974e19e093
- 出典データセット
- uspto-grants-1976_10