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HRID 1287906作成日：2026年10月25日

1-Methylazepan-4-one → 4-[2-(4,4-Dimethyl-2-oxazolin-2-yl)phenyl]-2,3,4,5,6,7-hexahydro-4-hydroxy-1-methylazepine

https://huagongshe.com/reaction/1287906

反応式

関与物質

役割名称HCID仕込み量
反応物1-Methylazepan-4-oneHCID 262586—
反応物2-(2-Bromophenyl)-4,4-dimethyl-4,5-dihydro-1,3-oxazoleHCID 289296—
生成物4-[2-(4,4-Dimethyl-2-oxazolin-2-yl)phenyl]-2,3,4,5,6,7-hexahydro-4-hydroxy-1-methylazepineHCID 21506815—

反応手順

Reaction of 2,3,4,5,6,7-hexahydro-1-methylazepin-4-one and 2-(2-bromophenyl)-4,4-dimethyl-2-oxazoline by the method described in Example 1c provides 4-[2-(4,4-dimethyl-2-oxazolin-2-yl)phenyl]-2,3,4,5,6,7-hexahydro-4-hydroxy-1-methylazepine.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US03985889
出典データセットuspto-grants-1976_10
ORD IDord-874686ac25474b30895ea07e188cbf55
出典メモuspto-grants-1976_10