関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzene | HCID 241 | — |
| 反応物 | Thiophosphoryl chloride | HCID 19883 | — |
| 生成物 | Phenylthionophosphonic dichloride | HCID 19016 | — |
反応手順
In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US03988368 |
|---|
| 出典データセット | uspto-grants-1976_10 |
|---|
| ORD ID | ord-3415756249a948d698066d8c2ad191f4 |
|---|
| 出典メモ | uspto-grants-1976_10 |
|---|
