Methyl isothiocyanate → HCID 10702319、化合物

HRID 1289774

反応式

HRID 1289774 の反応式
[NH2:1][C:2]1[N:6]=[C:5]([CH3:7])[NH:4][N:3]=1.[CH3:8][N:9]=[C:10]=[S:11]>CN(C)C=O>[NH2:1][C:2]1[N:3]([C:10]([NH:9][CH3:8])=[S:11])[N:4]=[C:5]([CH3:7])[N:6]=1

参加物

4

反応物 2

HCID 11167Methyl isothiocyanateHCID 2346103-Amino-5-methyl-4H-1,2,4-triazole

生成物 1

HCID 10702319HCID 10702319、化合物収率 29%

試薬・触媒・溶媒 1

HCID 6228Dimethylformamide溶媒

実験手順

The synthesis method of Example 1-(3) was applied. The compound (664 mg) obtained in (2) above, dimethylformamide (13 ml) and methyl isothiocyanate (600 mg) were used as reagents to give 340 mg of white crystals (yield 29%).

出典と根拠

ORDレコード
ord-49a7c28491a444d1a3f480263c3ca0df
出典データセット
uspto-grants-1998_05
特許番号
US05750545

関連ノート

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