Dimethylformamide → HCID 10725863、化合物
反応式
[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[NH:4][N:3]=1.CN(C)C=O.[CH3:13][N:14]=[C:15]=[S:16]>C(OCC)(=O)C>[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[N:4]([C:15]([NH:14][CH3:13])=[S:16])[N:3]=1参加物
5
実験手順
The synthesis method of Example 1-(3) was applied. 3,5-Diamino-1H-1,2,4-triazole (11.0 g), dimethylformamide (100 ml) and methyl isothiocyanate (10.0 g) were used as reagents. After the reaction, recrystallization from ethyl acetate gave 13.0 g of white powdery crystals (yield (68%).
出典と根拠
- ORDレコード
- ord-f71d34baffd24603867bf57e1aef3afa
- 出典データセット
- uspto-grants-1998_05
- 特許番号
- US05750545
反応ノート
読み込み中…