Methanol, 1,1-diethoxy-, 1-acetate → HCID 86752545、化合物
反応式
[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[N:4]([C:8]([NH:10][CH3:11])=[S:9])[N:3]=1.[C:12]([O:15][CH:16](OCC)OCC)(=O)[CH3:13]>>[NH2:7][C:5]1[N:4]([C:8]([NH:10][CH3:11])=[S:9])[N:3]=[C:2]([N:1]=[CH:16][O:15][CH2:12][CH3:13])[N:6]=1参加物
3
実験手順
A solution of the compound (500 mg) obtained in Example 31 and diethoxymethyl acetate (7 ml) was stirred at room temperature. After stirring for 1 hour, the resulting crystals were collected by filtration to give 480 mg of a white powdery solid (yield 73%).
後処理
- filtrationthe resulting crystals were collected by filtration
出典と根拠
- ORDレコード
- ord-05f19ef343e343f58909148af11092a2
- 出典データセット
- uspto-grants-1998_05
- 特許番号
- US05750545
反応ノート
読み込み中…