化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Dichloroethane → Methyl 3-(4-chlorophenyl)-2-propenoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dichloroethane | HCID 11 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 2-Propenoic acid, 3-(4-chlorophenyl)- | HCID 15371 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Methyl 3-(4-chlorophenyl)-2-propenoate | HCID 98955 | 95% |
反応手順
The synthesis method of Example 7-(1) was applied. 4-Chlorocinnamic acid (10.0 g), 1,2-dichloroethane (50 methanol (9.0 ml) and concentrated sulfuric acid (0.4 ml) were used as reagents to give 10.2 g of a white solid (yield 95%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05750545 |
| 出典データセット | uspto-grants-1998_05 |
| ORD ID | ord-0677265866c244d1aee9377bcdf37155 |
| 出典メモ | uspto-grants-1998_05 |