Methanol, 1,1-diethoxy-, 1-acetate → 2-[(N-Benzylidene)amino]-6-methyl-1,2,4-triazolo[1,5-a]-1,3,5-triazine-7 (6H)-thione
反応式
[NH2:1][C:2]1[N:6]([C:7]([NH:9][CH3:10])=[S:8])[N:5]=[C:4]([N:11]=[CH:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[N:3]=1.[C:19](OC(OCC)OCC)(=O)C>>[CH:12](=[N:11][C:4]1[N:3]=[C:2]2[N:1]=[CH:10][N:9]([CH3:19])[C:7](=[S:8])[N:6]2[N:5]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1参加物
3
実験手順
The synthesis method of Example 55 was applied. The compound (783 mg) obtained in Example 37 and diethoxymethyl acetate (5 ml) were used as reagents. The mixture was reacted at 90° C. for 1.5 hours to give 757 mg of white powdery crystals (yield 93%).
後処理
- customThe synthesis method of Example 55
- customThe mixture was reacted at 90° C. for 1.5 hours
出典と根拠
- ORDレコード
- ord-a8810adf3fba431d9f89cfd75ccdfe35
- 出典データセット
- uspto-grants-1998_05
- 特許番号
- US05750545
反応ノート
読み込み中…