化工社化工社 化学情報印刷レポート · 研究参考用
a Farnesol → 3,7,11-Trimethyldodeca-2,6,10-trienyl 2-phenylacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | a Farnesol | HCID 3327 | — |
| 反応物 | Phenylacetyl chloride | HCID 7679 | — |
| 生成物 | 3,7,11-Trimethyldodeca-2,6,10-trienyl 2-phenylacetate | HCID 54216610 | 54% |
反応手順
A mixture of farnesol (440 mg, 2 mmol) and phenylacetyl chloride (584 mg, 7.8 mmol) was refluxed for 2.5 hours. Extraction with hexane, and purification yielded 368 mg (yield: 54%) of oil having the following physical properties.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05466718 |
| 出典データセット | uspto-grants-1995_11 |
| ORD ID | ord-1d1526befd3a4af7a497eab7cf9d512e |
| 出典メモ | uspto-grants-1995_11 |