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Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester → cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester | HCID 86750331 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 溶媒 | Sodium methanolate methanol | HCID 23694274 | — |
| 生成物 | cis-(+/-)-5-(Azidomethyl)tetrahydro-3-furanthiol | HCID 86750332 | 64.8% |
反応手順
The title compound is prepared by the procedure of Example 16 using 0.310 g of product from Example 61 in 4.5 ml of tetrahydrofuran and 0.30 ml of 25% sodium methoxide/methyl alcohol to give 0.159 g of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05750735 |
| 出典データセット | uspto-grants-1998_05 |
| ORD ID | ord-eec246d0f4684cf9baba81883fabb9e3 |
| 出典メモ | uspto-grants-1998_05 |