4-Bromobutyronitrile → 4-(2-(11-Carbomethoxyundecanoylamino)phenoxy)-butyronitrile

反応式

[C:1]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]([NH:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[OH:24])=[O:16])([O:3][CH3:4])=[O:2].Br[CH2:26][CH2:27][CH2:28][C:29]#[N:30]>>[C:1]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]([NH:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[O:24][CH2:26][CH2:27][CH2:28][C:29]#[N:30])=[O:16])([O:3][CH3:4])=[O:2]

参加物

反応物 2

HCID 214124-Bromobutyronitrile

HCID 18795789N-(11-Carbomethoxyundecanoyl)-2-hydroxyaniline

生成物 1

HCID 196031824-(2-(11-Carbomethoxyundecanoylamino)phenoxy)-butyronitrile

実験手順

When (44) and 4-bromobutyronitrile are reacted under the conditions of step (A), above, (45) is obtained as a waxy solid. Conversely, reacting (44) with ethyl 4-bromobutyrate as in step (A) yields (8).

出典と根拠

ORDレコード: ord-c2872b9c066b45f7a67824d95c91311c
出典データセット: uspto-grants-1998_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05753641

反応ノート

読み込み中…