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M-Cresol → tert-Butyl 4-[(1S)-1-({[5-chloro-2-(3-methylphenoxy)pyridin-3-yl]carbonyl}amino)ethyl]benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | M-Cresol | HCID 342 | — |
| 反応物 | tert-butyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate | HCID 57572256 | — |
| 生成物 | tert-Butyl 4-[(1S)-1-({[5-chloro-2-(3-methylphenoxy)pyridin-3-yl]carbonyl}amino)ethyl]benzoate | HCID 69419528 | — |
反応手順
The title compound was prepared according to the procedure described in step 2 of Example 45 from tert-butyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 45) and m-cresol: MS (ESI) m/z 467 (M+H)+, 465 (M−H)−.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07238714B2 |
| 出典データセット | uspto-grants-2007_07 |
| ORD ID | ord-5391f91f6a104747a3df5e4f5137d13a |
| 出典メモ | uspto-grants-2007_07 |