化工社化工社 化学情報印刷レポート · 研究参考用
4-Bromophenol → p-Bromo-(1-methoxyethoxy)benzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Bromophenol | HCID 7808 | — |
| 反応物 | Methyl vinyl ether | HCID 7861 | — |
| 生成物 | p-Bromo-(1-methoxyethoxy)benzene | HCID 22908633 | 90% |
反応手順
Using p-bromophenol (17.3 g, 0.1 mole) and methyl vinyl ether (14.0 g, 0.2 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1), and the crude oil (24 g) was purified by distillation under reduced pressure to afford 20.8 g of p-bromo-(1-methoxyethoxy)benzene as a pale yellow oil having a boiling point 89-90° C./2 mmHg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05468589 |
| 出典データセット | uspto-grants-1995_11 |
| ORD ID | ord-24808c6fb6474ee0bab5996c316c4c25 |
| 出典メモ | uspto-grants-1995_11 |