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Isoprene → 2-Methylbuta-1,3-diene--2-methylprop-1-ene (1/1)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isoprene | HCID 6557 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2-Methylbuta-1,3-diene--2-methylprop-1-ene (1/1) | HCID 62703 | — |
反応手順
The methodology of Example 3 was repeated, except that 1.5 mL of isoprene was added to the reaction vessel prior to initiation. The mixture was allowed to stir at −78° C. for 10 minutes, before addition of methanol (10 mL) to terminate the reaction. The yield of copolymer was 5.5 g (Mn=104,000, Mw=203,000). The isoprene content in the rubber was 1.5 mol-percent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07238819B2 |
| 出典データセット | uspto-grants-2007_07 |
| ORD ID | ord-3c3de0c419514d8daadb65184fdf715d |
| 出典メモ | uspto-grants-2007_07 |