Cyclohexene → HCID 136358451、化合物
反応式
C[O:2][C:3]1[CH:8]=[C:7]([O:9]C)[CH:6]=[CH:5][C:4]=1[C:11]1[C:19]2[C:14](=[C:15]([C:20]([F:23])([F:22])[F:21])[CH:16]=[CH:17][CH:18]=2)[N:13]([CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])[N:12]=1.B(Br)(Br)Br.C1CCCCC=1>>[CH2:24]([N:13]1[C:14]2[C:19](=[CH:18][CH:17]=[CH:16][C:15]=2[C:20]([F:23])([F:22])[F:21])[C:11]([C:4]2[CH:5]=[CH:6][C:7]([OH:9])=[CH:8][C:3]=2[OH:2])=[N:12]1)[CH2:25][CH2:26][CH2:27][CH3:28]参加物
4
実験手順
Prepared according to Method D step C from 3-(2,4-dimethoxyphenyl)-1-pentyl-7-(trifluoromethyl)-1H-indazole (0.055 g, 0.14 mmol), boron tribromide (0.136 mL, 1.4 mmol) and 1.0 mL of cyclohexene to give the product (0.048 g) as a white solid.
後処理
- customPrepared
出典と根拠
- ORDレコード
- ord-93a874ae17b24d8f8f6d4e0df4733b5e