化工社化工社 化学情報印刷レポート · 研究参考用
Ethylamine → 2-Chloro-N-ethyl-5-hydroxybenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylamine | HCID 6341 | — |
| 反応物 | 2-Chloro-5-hydroxybenzoic acid | HCID 458210 | — |
| 生成物 | 2-Chloro-N-ethyl-5-hydroxybenzamide | HCID 58907486 | — |
反応手順
The title compound was prepared from 2-chloro-5-hydroxybenzoic acid and ethylamine, using a method similar to that used for preparation 52, as a colourless solid. 1HNMR (400 MHz, CDCl3) δ: 1.22 (3H, t), 3.42–3.49 (2H, m), 6.48–6.52 (1H, m), 6.80 (1H, dd), 7.13 (1H, d), 7.38 (1H, d); LRMS ESI m/z 200 [M+H]+
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07241810B2 |
| 出典データセット | uspto-grants-2007_07 |
| ORD ID | ord-1887cb4f412d407db3003ab77cc1f53a |
| 出典メモ | uspto-grants-2007_07 |