Methylamine → 6-Hydroxy-N-methyl-1-naphthamide

HRID 1295906ノート

反応式

HRID 1295906 の反応式
[OH:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[C:8]([C:12]([OH:14])=O)=[CH:7][CH:6]=[CH:5]2.[CH3:15][NH2:16]>>[OH:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[C:8]([C:12]([NH:16][CH3:15])=[O:14])=[CH:7][CH:6]=[CH:5]2

参加物

3

反応物 2

HCID 6329MethylamineHCID 54638006-Hydroxy-1-naphthoic acid

生成物 1

HCID 228927966-Hydroxy-N-methyl-1-naphthamide

実験手順

Prepared from 6-hydroxy-1-naphthoic acid and methylamine using the method of preparation 57 to give the title compound as a pale orange solid.

後処理

  1. customthe method of preparation 57

出典と根拠

ORDレコード
ord-da0ab6c8017e4fb294d24fca8eebc3eb
出典データセット
uspto-grants-2007_07
特許番号
US07244766B2

反応ノート

読み込み中…