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Acetic Anhydride → N-(hydroxymethyl)acetamide acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | Formicin | HCID 69365 | — |
| 触媒 | Pyridine | HCID 1049 | — |
| 生成物 | N-(hydroxymethyl)acetamide acetate | HCID 86745977 | 900% |
反応手順
Acetic anhydride (25 g) and pyridine (10 drops) is added to N-(hydroxymethyl)acetamide (9 g, 0.1 mol). The reaction mixture is stirred overnight at room temperature, concentrated in vacuo and chased with xylene to give the title product as an oil (11.9 g, 0.9 mol) which is identified by 1HNMR spectral analysis.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05468877 |
| 出典データセット | uspto-grants-1995_11 |
| ORD ID | ord-7c0bd3edec95447594664c9e2887776d |
| 出典メモ | uspto-grants-1995_11 |