化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → Allyl 2-fluoro-4-hydroxybenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Allyl Alcohol | HCID 7858 | — |
| 反応物 | 2-Fluoro-4-hydroxybenzoic Acid | HCID 2783398 | — |
| 生成物 | Allyl 2-fluoro-4-hydroxybenzoate | HCID 14852522 | 69% |
反応手順
In a manner analogous to Example 1(a), starting with 8.3 g (53 mmoles) of 2-fluoro-4-hydroxybenzoic acid treated for 2 hours at 100° C. with 60 ml of allyl alcohol and 1.5 ml of concentrated sulfuric acid, 7.2 g (69% yield) of the expected ester having a melting point of 80°-81° C. are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05468897 |
| 出典データセット | uspto-grants-1995_11 |
| ORD ID | ord-03abb826f4a64626b71d362af898e2c2 |
| 出典メモ | uspto-grants-1995_11 |