化工社化工社 化学情報印刷レポート · 研究参考用
Allyl Alcohol → Allyl 4-hydroxy-3-methoxybenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Allyl Alcohol | HCID 7858 | — |
| 反応物 | Vanillic Acid | HCID 8468 | — |
| 溶媒 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | Allyl 4-hydroxy-3-methoxybenzoate | HCID 11117259 | 75% |
反応手順
In a manner analogous to Example 1(a), 5 g (30 mmoles) of 4-hydroxy-3-methoxybenzoic acid treated at 100° C. for 4 hours with 50 ml of allyl alcohol and 820 μl of concentrated sulfuric acid, give 4.65 g (75% yield) of the expected ester in the form of a slightly yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05468897 |
| 出典データセット | uspto-grants-1995_11 |
| ORD ID | ord-877c07731dfd4847a8cf610d152a9e72 |
| 出典メモ | uspto-grants-1995_11 |