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2-Acetylnaphthalene → 4,4,5,5,6,6,6-Heptafluoro-1-(2-naphthyl)hexane-1,3-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Acetylnaphthalene | HCID 7122 | — |
| 反応物 | Butanoic acid, 2,2,3,3,4,4,4-heptafluoro-, ethyl ester | HCID 9644 | — |
| 生成物 | 4,4,5,5,6,6,6-Heptafluoro-1-(2-naphthyl)hexane-1,3-dione | HCID 86004327 | — |
反応手順
The compound was synthesized according to example 1 using 2-acetylnaphthalene and ethyl heptafluorobutyrate as starting materials. The product was crystallized from petroleum ether. 1H NMR (CDCl3): 6.76 (s, 1 H); 7.57-7.66 (m, 2H); 7.90 (bd, 1 H); 7.93-7.94 (m, 2H); 7.98 (bd, 1 H); 8.53 (s, 1H). IR (film): 1602 (C═O); 1232 (C—F).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07381567B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-ed593dcb2091417f8386ebc40775ec71 |
| 出典メモ | uspto-grants-2008_06 |