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N-(3,4-Dichlorophenyl)thiourea → (3,4-Dichloro-phenyl)-[4-(4-methanesulfonyl-phenyl)-thiazol-2-yl]-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(3,4-Dichlorophenyl)thiourea | HCID 710776 | — |
| 反応物 | 2-Bromo-4'-(methylsulfonyl)acetophenone | HCID 735823 | — |
| 生成物 | (3,4-Dichloro-phenyl)-[4-(4-methanesulfonyl-phenyl)-thiazol-2-yl]-amine | HCID 32253410 | 78% |
反応手順
(3,4-Dichloro-phenyl)-[4-(4-methanesulfonyl-phenyl)-thiazol-2-yl]-amine was prepared in 78% yield using the procedure described in example 31 from 2-Bromo-1-(4-methanesulfonyl-phenyl)-ethanone and (3,4-Dichloro-phenyl)-thiourea. 1H NMR (300 MHz, DMSO-d6) δ 8.16-7.56 (m, 8H), 3.24 (s, 3H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07381736B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-d8b297154fbb4023a7544f427b415052 |
| 出典メモ | uspto-grants-2008_06 |